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Abstract | Cited by

A continuous-flow protocol for the synthesis of diazo acetonitrile was developed. It was further applied in iron-catalysed insertion reactions of diazo acetonitrile into N–H and S–H bonds to yield valuable α-substituted acetonitrile, including gram-scale synthesis.

Graphical abstract: Iron-catalysed carbene-transfer reactions of diazo acetonitrile

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