Issue 4, 1973

Preparation of 1,3,2-benzodithiaphospholes and the X-ray crystal structure of 2-methyl-2,2′-spirobi-(1,3,2-benzodithiaphosphole)

Abstract

A series of monocyclic and spiro 1,3,2-benzodithiaphospholes (C6H4S2)PRnF3–n(n[double bond, length as m-dash]2, R[double bond, length as m-dash]Ph, Me), (n= 3, R = Pri) and (C6H4S2)2PR (R = Ph, Me) have been synthesised and the structure of one of these, (C6H4S2)2PMe, has been determined by X-ray diffraction.

Article information

Article type
Paper

J. Chem. Soc., Chem. Commun., 1973, 144-145

Preparation of 1,3,2-benzodithiaphospholes and the X-ray crystal structure of 2-methyl-2,2′-spirobi-(1,3,2-benzodithiaphosphole)

M. Eisenhut, R. Schmutzler and W. S. Sheldrick, J. Chem. Soc., Chem. Commun., 1973, 144 DOI: 10.1039/C39730000144

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