Preparation of the optically pure alkylation reagent (3) and its reaction with Grignard and alkyl-lithium reagents provides a general route to iron alkyls whose enantiomeric purity may be shown by the n.m.r. spectra of their SO2 insertion products.
T. C. Flood, F. J. DiSanti and D. L. Miles, J. Chem. Soc., Chem. Commun., 1975, 336 DOI: 10.1039/C39750000336
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