Isotope incorporation studies on the base hydrolysis of the methanesulphonic anhydrides of phosphinothioic acids (1) using 18O enriched water and D2O have shown that S–O bond cleavage occurs via a sulphene intermediate.
J. Michalski, C. Radziejewski and Z. Skrzypczyński, J. Chem. Soc., Chem. Commun., 1976, 762 DOI: 10.1039/C39760000762
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