Issue 15, 1977

X-Ray crystal structure of the novel bis-quaternary dispiro system obtained from the reaction of morpholine with hexakis(bromomethyl)benzene

Abstract

In contrast to the six-fold substitution of hexakis(bromomethyl)benzene (Ia) by aniline to give the hexa-amine (Ib), reaction of (Ia) with morpholine occurs with dispiro-annelation yielding (II); the structure of this novel product was deduced spectroscopically and its detailed molecular geometry was determined by X-ray crystallography.

Article information

Article type
Paper

J. Chem. Soc., Chem. Commun., 1977, 525-526

X-Ray crystal structure of the novel bis-quaternary dispiro system obtained from the reaction of morpholine with hexakis(bromomethyl)benzene

A. D. U. Hardy, D. D. MacNicol and D. R. Wilson, J. Chem. Soc., Chem. Commun., 1977, 525 DOI: 10.1039/C39770000525

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