X-Ray crystallographic studies of the anions [Sc(NO3)5]2– and [Y(NO3)5]2–, which have been prepared using liquid N2O4, have revealed novel co-ordination numbers of nine for scandium(III) and ten for yttrium(III), with geometries best described in terms of a pseudotrigonal bipyramid.
C. C. Addison, A. J. Greenwood, M. J. Haley and N. Logan, J. Chem. Soc., Chem. Commun., 1978, 580 DOI: 10.1039/C39780000580
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