Assignment of carbon-13 n.m.r. spectra by selective saturation
Abstract
Selective radio frequency saturation allied to gated proton decoupling and Fourier transform difference spectroscopy is used to give separate fully coupled 13C n.m.r. spectra from inividual carbon sites, and so aid the assignment of the spectrum of methyl 2,3-di-O-allyl-α-D-glucopyranoside.