Dioxabicyclo[n.2.1]alkanes bearing a cis-bromine on the one-carbon bridge are readily prepared from cycloalkenes by the sequence singlet oxygenation, bromination, and treatment with silver trifluoroacetate.
A. J. Bloodworth and H. J. Eggelte, J. Chem. Soc., Chem. Commun., 1979, 741 DOI: 10.1039/C39790000741
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