Adducts of thia-donors have been prepared as single crystals by a new galvanostatic electrocrystallisation method usually yielding better products than the potentiostatic method, although TTTI0·72(TTT = tetrathiatetracene) from the latter shows a metallic conductivity of 1·1 × 103Ω–1 cm–1 at 300 K.
P. Kathirgamanathan and D. R. Rosseinsky, J. Chem. Soc., Chem. Commun., 1980, 356 DOI: 10.1039/C39800000356
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