The [graphic omitted]+BF4– radical with the unpaired electron in an apical position of the trigonal-bipyramidal (TBP) structure is generated by X-irradiation via an intermediate TBP structure in which the unpaired electron is located in an equatorial position.
J. H. H. Hamerlinck, P. Schipper and H. M. Buck, J. Chem. Soc., Chem. Commun., 1981, 1148 DOI: 10.1039/C39810001148
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