The 23Na n.m.r. spectrum of the sodium anion in solutions of sodium in hexamethylphosphoric triamide is reported, and gives the first direct indication of a genuine sodium anion formed in a metal solution without added cation-complexing agents.
P. P. Edwards, S. C. Guy, D. M. Holton and W. McFarlane, J. Chem. Soc., Chem. Commun., 1981, 1185 DOI: 10.1039/C39810001185
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