Boron-11/proton two-dimensional n.m.r. spectroscopy with heteronuclear decoupling in both frequency dimensions has been used to study decaborane. The chemical-shift correlation map shows clearly how resonances from the various boron and proton sites are related, and in particular demonstrates the association of the bridging protons with B5,7,8,10 and with B6,9.
I. J. Colquhoun and W. McFarlane, J. Chem. Soc., Dalton Trans., 1981, 2014 DOI: 10.1039/DT9810002014
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