A new synthesis of methylenomycin B (3) has been accomplished in four steps starting with the reaction of methyl (E)-3-lithio-2-methyl-3-phenylthioprop-2-enoate (2) with ethyl 2-(phenylthiomethyl)prop-2-enoate (4).
Y. Takahashi, H. Kosugi and H. Uda, J. Chem. Soc., Chem. Commun., 1982, 496 DOI: 10.1039/C39820000496
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