The removal of aluminium from the zeolite framework of the ammonium form of synthetic faujasite during calcination has been observed using solid-state 29Si n.m.r. spectroscopy.
I. E. Maxwell, W. A. van Erp, G. R. Hays, T. Couperus, R. Huis and A. D. H. Clague, J. Chem. Soc., Chem. Commun., 1982, 523 DOI: 10.1039/C39820000523
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