Ethyl 3,5-dimethylorsellinate (3) doubly labelled with 13C and 18O in the carbonyl of the carboxy group and at the C-6 position has been synthesised using a four-step procedure from sodium [1-13C, 18O2]acetate, and incorporated into austin (1) by cultures of Aspergillus ustus.
F. E. Scott, T. J. Simpson, L. A. Trimble and J. C. Vederas, J. Chem. Soc., Chem. Commun., 1986, 214 DOI: 10.1039/C39860000214
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