The in situ generated chloromethyl-lithium reacts at –78 °C with different aldehydes and ketones to afford, after lithiation with lithium powder, terminal and exocyclic olefins.
J. Barluenga, J. L. Fernández-Simón, J. M. Concellón and M. Yus, J. Chem. Soc., Chem. Commun., 1986, 1665 DOI: 10.1039/C39860001665
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