High-resolution 31P solid-state NMR measurements on frozen solutions of a cyclic nucleotide (adenosine 3′,5′-cyclic monophosphate, sodium salt) provide the 31P shielding tensor and reveal that the chemical shift has a significant dependence upon hydrogen bonding.
I. P. Gerothanassis, P. J. Barrie and C. Tsanaktsidis, J. Chem. Soc., Chem. Commun., 1994, 2639 DOI: 10.1039/C39940002639
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