The synthesis of tris-ketol phosphates by the treatment of phosphoric acid–p-(difluoroiodo)toluene mixtures with silyl enol ethers and their conversion into lithium bis-ketol phosphates by the action of lithium bromide in acetone are described.
G. F. Koser, K. Chen, Y. Huang and C. A. Summers, J. Chem. Soc., Perkin Trans. 1, 1994, 1375 DOI: 10.1039/P19940001375
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