The use of a tandem Ireland Claisen rearrangement followed by an in situ silicon mediated epoxide fragmentation provides an efficient entry into 1,3-dienes containing an E-double bond and an exo-methylene group; initial results regarding remote chirality control are reported.
J. J. Eshelby, P. J. Parsons, N. C. Sillars and P. J. Crowley, J. Chem. Soc., Chem. Commun., 1995, 1497 DOI: 10.1039/C39950001497
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