The crystal structures of Et3N and Pri3N were determined by X-ray analysis using the in situ crystallization technique for single crystal growth on the diffractometer; both have a pyramidal configuration of the nitrogen atom, even Pri3N, which was considered to be planar in accord with electron diffraction and NMR data.
R. Boese, D. Bläser, M. Y. Antipin, R. Boese, M. Y. Antipin, V. Chaplinski and A. de Meijere, Chem. Commun., 1998, 781 DOI: 10.1039/A708399H
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