Reduction of [ButP]4 with K metal (1:5 equiv.) followed by the addition of pmdeta and stoichiometric hydrolysis gives [{(ButP)2H}K·pmdeta]2, a unique complex containing a [ButP(H)PBut]– anion ligand homologous with a phosphido anion (R2P–).
M. A. Beswick, A. D. Hopkins, L. C. Kerr, M. E. G. Mosquera, J. S. Palmer, P. R. Raithby, A. Rothenberger, A. E. H. Wheatley, D. S. Wright, D. Stalke and A. Steiner, Chem. Commun., 1998, 1527 DOI: 10.1039/A803834A
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