3-Methylthiophene can be synthesised in yields >95 mol% from the reaction of 2-methylbutanol and CS2 over MgO-supported potassium-promoted ‘Fe0.95Cr0.05OOK’; catalysts using γ-Al2O3 or other alkaline earth oxides as supports are less effective.
B. W. L. Southward, L. S. Fuller, R. A. Stewart, G. J. Hutchings and R. W. Joyner, Chem. Commun., 1999, 369 DOI: 10.1039/A809675I
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