Issue 8, 2003
From the journal:

Chemical Communications

Phase-transfer alkylation reactions using microreactors

Masaharu Ueno,a   Hideaki Hisamoto,b   Takehiko Kitamorib  and  Shū Kobayashi*a  

* Corresponding authors

a Graduate School of Pharmaceutical Sciences, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo, 113-0033, Japan
E-mail: skobayas@mol.f.u-tokyo.ac.jp
Fax: +81 3 5684 0634
Tel: +81 3 5841 4790

b Department of Applied Chemistry, Graduate School of Engineering, The University of Tokyo, 7-3-1 Hongo, Bunkyo-ku, Tokyo, 113-8656, Japan

Abstract

Phase-transfer alkylation in a microreactor proceeds smoothly, and the reaction has been found to be more efficient than that in a round-bottomed flask with vigorous stirring; we have observed by an optical microscope study that an interfacial area provided by organic and aqueous phases is more extended in a microreactor.

Graphical abstract: Phase-transfer alkylation reactions using microreactors

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Article information

DOI
https://doi.org/10.1039/B301638B
Article type
Communication
Submitted
12 Feb 2003
Accepted
05 Mar 2003
First published
27 Mar 2003

Chem. Commun., 2003, 936-937

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Phase-transfer alkylation reactions using microreactors

M. Ueno, H. Hisamoto, T. Kitamori and S. Kobayashi, Chem. Commun., 2003, 936 DOI: 10.1039/B301638B

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