Issue 21, 2003
From the journal:

Chemical Communications

Extended X-ray absorption fine structure (EXAFS) characterisation of dilute palladium homogeneous catalysts†

Steven G. Fiddy,*ab   John Evans,*a   Mark A. Newton,a   Thomas Neisius,b   Robert P. Toozec  and  Richard Oldmanc  

* Corresponding authors

a Department of Chemistry, The University of Southampton, Highfield, Southampton, UK
E-mail: je@soton.ac.uk

b ESRF, PO Box 220, Grenoble Cedex, F-38043, France
E-mail: fiddy@esrf.fr

c ICI-Synetix, PO Box 1, Belasis Ave, Billingham, UK

Abstract

Highly dilute EXAFS characterisation for the elucidation of species involved in Heck chemistry is demonstrated; the major “monomer” species of Herrmann's acetate-bridged phosphapalladadacycle is characterised and species present during the course of a 50 ppm [Pd] Pd(OAc)2/PBut3 catalysed Heck reaction are presented.

Graphical abstract: Extended X-ray absorption fine structure (EXAFS) characterisation of dilute palladium homogeneous catalysts

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Article information

DOI
https://doi.org/10.1039/B307535D
Article type
Communication
Submitted
02 Jul 2003
Accepted
09 Sep 2003
First published
24 Sep 2003

Chem. Commun., 2003, 2682-2683

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Extended X-ray absorption fine structure (EXAFS) characterisation of dilute palladium homogeneous catalysts

S. G. Fiddy, J. Evans, M. A. Newton, T. Neisius, R. P. Tooze and R. Oldman, Chem. Commun., 2003, 2682 DOI: 10.1039/B307535D

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