Issue 14, 2005
From the journal:

Chemical Communications

Anhydrous solution synthesis of germanium nanocrystals from the germanium(ii) precursor Ge[N(SiMe3)2]2†

Henry Gerung,a   Scott D. Bunge,b   Timothy J. Boyle,*b   C. Jeffrey Brinkerab  and  Sang M. Hana  

* Corresponding authors

a Department of Chemical and Nuclear Engineering, University of New Mexico, 209 Farris Engineering Center, Albuquerque, NM 87131, USA
E-mail: meister@unm.edu
Fax: +1 505-277-5433
Tel: +1 505-277-3118

b Advanced Materials Laboratory, Sandia National Laboratories, 1001 University Boulevard SE, Albuquerque, NM 87106, USA
E-mail: tjboyle@sandia.gov
Fax: +1 505-272-7336
Tel: +1 505-272-7625

Abstract

A convenient, simple, single-source solution synthesis of Ge nanocrystals via thermal reduction of Ge(II) precursor Ge[N(SiMe3)2]2 in a non-coordinating solvent at 300 °C and 1 atm Ar is described.

Graphical abstract: Anhydrous solution synthesis of germanium nanocrystals from the germanium(ii) precursor Ge[N(SiMe3)2]2

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Article information

DOI
https://doi.org/10.1039/B416066E
Article type
Communication
Submitted
18 Oct 2004
Accepted
01 Feb 2005
First published
16 Feb 2005

Chem. Commun., 2005, 1914-1916

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Anhydrous solution synthesis of germanium nanocrystals from the germanium(II) precursor Ge[N(SiMe3)2]2

H. Gerung, S. D. Bunge, T. J. Boyle, C. J. Brinker and S. M. Han, Chem. Commun., 2005, 1914 DOI: 10.1039/B416066E

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