Rapid one-pot synthesis of LiMPO4 (M = Fe, Mn) colloidal nanocrystals by supercritical ethanol process

Dinesh Rangappa; Koji Sone; Masaki Ichihara; Tetsuichi Kudo; Itaru Honma

doi:10.1039/C0CC03034A

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Rapid one-pot synthesis of LiMPO₄ (M = Fe, Mn) colloidal nanocrystals by supercritical ethanol process†

Dinesh Rangappa,*^ab Koji Sone,^b Masaki Ichihara,^c Tetsuichi Kudo^b and Itaru Honma*^ab

Author affiliations

* Corresponding authors

^a Multidisciplinary Research for Advanced Materials, Tohoku University, 2-1-1 Katahira, Aoba-ku, Sendai 980-8577, Japan
E-mail: dineshrangappa@gmail.com, i.honma@tagen.tohoku.ac.jp

^b ETRI, National Institute of Advanced Industrial Science and Technology AIST, Umezono 1-1-1, Tsukuba, Ibaraki 305-8568, Japan

^c Material Design and Characterization Laboratory, ISSP, University of Tokyo, 5-1-5 Kashiwanoha, Kashiwa, Chiba 277-8581, Japan

Abstract

We report a rapid one-pot supercritical fluid approach to prepare the desired size and morphology controlled LiMPO₄ nanocrystals, using oleylamine as both capping and reducing agent.

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Supplementary files

Experimental section PDF (2052K)

Article information

DOI: https://doi.org/10.1039/C0CC03034A
Article type: Communication
Submitted: 04 Aug 2010
Accepted: 03 Sep 2010
First published: 17 Sep 2010

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Chem. Commun., 2010,46, 7548-7550

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Rapid one-pot synthesis of LiMPO₄ (M = Fe, Mn) colloidal nanocrystals by supercritical ethanol process

D. Rangappa, K. Sone, M. Ichihara, T. Kudo and I. Honma, Chem. Commun., 2010, 46, 7548 DOI: 10.1039/C0CC03034A

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