Issue 7, 2010
From the journal:

CrystEngComm

Efficient Havinga–Kondepudi resolution of conglomerate amino acid derivatives by slow cooling and abrasive grinding†

Michel Leeman,a   Wim L. Noorduin,b   Alessia Millemaggi,c   Elias Vlieg,b   Hugo Meekes,b   Willem J. P. van Enckevort,b   Bernard Kapteinc  and  Richard M. Kellogg*a  

* Corresponding authors

a Syncom BV, Kadijk 3, Groningen, The Netherlands
E-mail: r.m.kellogg@syncom.nl
Fax: +31 (0)50 5757399
Tel: +31 (0)50 5757272

b IMM Solid State Chemistry, Radboud University Nijmegen, Heyendaalseweg 135, Nijmegen, The Netherlands

c DSM Innovative Synthesis BV, PO Box 18, Geleen, The Netherlands

Abstract

The complete resolution of the conglomerate racemates of two amino acid derivatives susceptible to racemization in solution was achieved by slow crystallization from a supersaturated solution accompanied by cooling and abrasive grinding.

Graphical abstract: Efficient Havinga–Kondepudi resolution of conglomerate amino acid derivatives by slow cooling and abrasive grinding

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Article information

DOI
https://doi.org/10.1039/C0CE00140F
Article type
Communication
Submitted
16 Apr 2010
Accepted
04 May 2010
First published
25 May 2010

CrystEngComm, 2010,12, 2051-2053

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Efficient Havinga–Kondepudi resolution of conglomerate amino acid derivatives by slow cooling and abrasive grinding

M. Leeman, W. L. Noorduin, A. Millemaggi, E. Vlieg, H. Meekes, W. J. P. van Enckevort, B. Kaptein and R. M. Kellogg, CrystEngComm, 2010, 12, 2051 DOI: 10.1039/C0CE00140F

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