Issue 66, 2012
From the journal:

Chemical Communications

Low temperature solventless synthesis and characterization of Ni and Fe magnetic nanoparticles†

Liis Seinberg,a   Shinpei Yamamoto,*b   Ruwan Gallage,bc   Masahiko Tsujimoto,b   Yoji Kobayashi,a   Seiji Isoda,b   Mikio Takanob  and  Hiroshi Kageyamaabd  

* Corresponding authors

a Department of Energy and Hydrocarbon Chemistry, Graduate School of Engineering, Kyoto University, Nishikyo-ku, Kyoto, Japan

b Institute for Integrated Cell-Material Sciences, Kyoto University, Yoshida-Ushinomiyacho, Sakyo-ku, Kyoto, Japan
E-mail: yamamoto@icems.kyoto-u.ac.jp
Fax: +81-75-383-2510
Tel: +81-75-383-2513

c Toda Kogyo, Corp., 1-4, Meijishinkai, Otake, Hiroshima, Japan

d CREST, Japan Science and Technology Agency (JST), Japan

Abstract

We have successfully implemented a facile, one-pot solventless synthesis procedure starting from acetylacetonate salts and CaH2 to obtain carbon-coated ferromagnetic metallic Ni and Fe nanoparticles at low temperature. The use of CaH2 as a reductant drastically reduces reaction temperature down to 140 °C.

Graphical abstract: Low temperature solventless synthesis and characterization of Ni and Fe magnetic nanoparticles

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Article information

DOI
https://doi.org/10.1039/C2CC33830K
Article type
Communication
Submitted
29 May 2012
Accepted
02 Jul 2012
First published
03 Jul 2012

Chem. Commun., 2012,48, 8237-8239

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Low temperature solventless synthesis and characterization of Ni and Fe magnetic nanoparticles

L. Seinberg, S. Yamamoto, R. Gallage, M. Tsujimoto, Y. Kobayashi, S. Isoda, M. Takano and H. Kageyama, Chem. Commun., 2012, 48, 8237 DOI: 10.1039/C2CC33830K

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