Issue 58, 2013
From the journal:

Chemical Communications

Electrochemical synthesis of azanucleoside derivatives using a lithium perchlorate–nitromethane system†

Shokaku Kim,a   Takao Shoji,a   Yoshikazu Kitanoa  and  Kazuhiro Chiba*a  

* Corresponding authors

a Laboratory of Bio-organic Chemistry, Tokyo University of Agriculture and Technology, 3-5-8 Saiwai-cho, Fuchu, Tokyo 183-8509, Japan
E-mail: chiba@cc.tuat.ac.jp
Fax: +81 42 360 7167
Tel: +81 42 367 5667

Abstract

We have developed a highly efficient synthetic method for azanucleosides using a lithium perchlorate–nitromethane reaction medium, allowing direct and exclusive installation of various nucleophiles, including protected nucleobases into prolinol derivatives at the preferred 5-position.

Graphical abstract: Electrochemical synthesis of azanucleoside derivatives using a lithium perchlorate–nitromethane system

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Article information

DOI
https://doi.org/10.1039/C3CC43273D
Article type
Communication
Submitted
03 May 2013
Accepted
26 May 2013
First published
30 May 2013

Chem. Commun., 2013,49, 6525-6527

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Electrochemical synthesis of azanucleoside derivatives using a lithium perchlorate–nitromethane system

S. Kim, T. Shoji, Y. Kitano and K. Chiba, Chem. Commun., 2013, 49, 6525 DOI: 10.1039/C3CC43273D

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