Issue 33, 2013

DMAP mediated one-pot domino thienannulation: a versatile, regioselective and green mechanochemical route to naphtho[2,3-b]thiophenes

Abstract

Solvent-free mechanochemical route to naphtho[2,3-b]thiophenes via [3 + 2] oxidative heteroannulation of α-enolicdithioesters and β-oxothioamides with 1,4-naphthoquinone has been achieved at room temperature.

Graphical abstract: DMAP mediated one-pot domino thienannulation: a versatile, regioselective and green mechanochemical route to naphtho[2,3-b]thiophenes

Supplementary files

Article information

Article type
Paper
Submitted
07 Mar 2013
Accepted
09 May 2013
First published
09 May 2013

RSC Adv., 2013,3, 13811-13817

DMAP mediated one-pot domino thienannulation: a versatile, regioselective and green mechanochemical route to naphtho[2,3-b]thiophenes

G. Shukla, G. K. Verma, A. Nagaraju, R. K. Verma, K. Raghuvanshi and M. S. Singh, RSC Adv., 2013, 3, 13811 DOI: 10.1039/C3RA41100A

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