Hydroformylation of alkynes is an underdeveloped atom-economic and redox-neutral method to prepare enals. Applying a new electron poor self-assembling ligand system provides the first general rhodium-catalyst for the chemo- and stereoselective hydroformylation of dialkyl- as well as diaryl-substituted alkynes to furnish enals in excellent chemo- and stereoselectivity.
V. Agabekov, W. Seiche and B. Breit, Chem. Sci., 2013, 4, 2418 DOI: 10.1039/C3SC50725D
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