Issue 8, 2014
From the journal:

Chemical Communications

Probing 27Al–13C proximities in metal–organic frameworks using dynamic nuclear polarization enhanced NMR spectroscopy†

Frédérique Pourpoint,*a   Aany Sofia Lilly Thankamony,a   Christophe Volkringer,a   Thierry Loiseau,a   Julien Trébosc,a   Fabien Aussenac,b   Diego Carnevale,c   Geoffrey Bodenhausen,cd   Hervé Vezin,e   Olivier Lafon*a  and  Jean-Paul Amoureuxaf  

* Corresponding authors

a Université Lille Nord de France, CNRS, UMR 8181 UCCS, ENSCL, Université de Lille 1, 59652 Villeneuve d'Ascq, France
E-mail: frederique.pourpoint@ensc-lille.fr, olivier.lafon@univ-lille1.fr
Tel: +33 320436542

b Bruker BioSpin SA, 34, rue de l'Industrie, 67166 Wissembourg Cedex, France

c Institut des sciences et ingénierie chimiques, Ecole Polytechnique Fédérale de Lausanne, EPFL, Batochime, CH-1015 Lausanne, Switzerland

d Département de chimie, Ecole Normale Supérieure, 24, rue Lhomond, 75321 Paris cedex 05, France

e Université Lille Nord de France, CNRS, UMR LASIR 8516, Université de Lille 1, 59652 Villeneuve d'Ascq, France

f East China Normal University, Shanghai, China

Abstract

We show how 27Al–13C proximities in the microporous metal–organic framework MIL-100(Al) can be probed using advanced 27Al–13C NMR methods boosted by Dynamic Nuclear Polarization.

Graphical abstract: Probing 27Al–13C proximities in metal–organic frameworks using dynamic nuclear polarization enhanced NMR spectroscopy

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Article information

DOI
https://doi.org/10.1039/C3CC47208F
Article type
Communication
Submitted
20 Sep 2013
Accepted
14 Nov 2013
First published
15 Nov 2013

Chem. Commun., 2014,50, 933-935

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Probing 27Al–13C proximities in metal–organic frameworks using dynamic nuclear polarization enhanced NMR spectroscopy

F. Pourpoint, A. S. L. Thankamony, C. Volkringer, T. Loiseau, J. Trébosc, F. Aussenac, D. Carnevale, G. Bodenhausen, H. Vezin, O. Lafon and J. Amoureux, Chem. Commun., 2014, 50, 933 DOI: 10.1039/C3CC47208F

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