The lithium–oxygen (Li–O2) electrochemical reaction on nanoporous gold (NPG) is observed using in situ atomic force microscopy (AFM) imaging coupled with potentiostatic measurement. Dense Li2O2 nanoparticles form a film at 2.5 V, which is decomposed at 3.8–4.0 V in an ether-based electrolyte.
R. Wen and H. R. Byon, Chem. Commun., 2014, 50, 2628 DOI: 10.1039/C3CC49625B
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