Issue 6, 2014
From the journal:

Green Chemistry

Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/bromides using oxone-KX (X = Cl or Br) in water†

Sridhar Madabhushi,*a   Raveendra Jillella,a   Vinodkumar Sriramojua  and  Rajpal Singhb  

* Corresponding authors

a Fluoroorganics Division, CSIR-Indian Institute of Chemical Technology, Hyderabad-500007, India
E-mail: smiict@gmail.com
Fax: +91 40 27160387
Tel: +91 40 27191772

b Centre for Fire Explosives and Environmental Safety, DRDO, Timarpur, New Delhi-110054, India

Abstract

A simple and rapid method for efficient synthesis of sulfonyl chlorides/bromides by oxyhalogenation of thiols and disulfides with oxone-KX (X = Cl or Br) using water as the solvent is described.

Graphical abstract: Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/bromides using oxone-KX (X = Cl or Br) in water

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Article information

DOI
https://doi.org/10.1039/C4GC00246F
Article type
Paper
Submitted
13 Feb 2014
Accepted
21 Mar 2014
First published
21 Mar 2014

Green Chem., 2014,16, 3125-3131

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Oxyhalogenation of thiols and disulfides into sulfonyl chlorides/bromides using oxone-KX (X = Cl or Br) in water

S. Madabhushi, R. Jillella, V. Sriramoju and R. Singh, Green Chem., 2014, 16, 3125 DOI: 10.1039/C4GC00246F

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