We report herein a light-mediated, palladium-catalyzed cyclization of unactivated 1,6-dienes under UV irradiation at rt. 1,5-Dimethylcyclopent-1-enes are formed as the only product in this transformation in moderate to excellent yields. This reaction offers a new insight into the realization of photochemical access to monocycles under ambient conditions.
W. Du, G. Tang, Y. Chen, D. Xu and H. Guo, Org. Chem. Front., 2014, 1, 919 DOI: 10.1039/C4QO00145A
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