We demonstrate the acquisition of ultrafast 2D NMR spectra of semi-solid samples, with a high-resolution magic-angle-spinning setup. Using a recent double-quantum NMR pulse sequence in optimised synchronisation conditions, high-quality 2D spectra can be recorded for a sample under magic-angle spinning. An illustration is given with a semi-solid sample of banana pulp.
M. André, M. Piotto, S. Caldarelli and J. Dumez, Analyst, 2015, 140, 3942 DOI: 10.1039/C5AN00653H
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