An efficient and high-yielding synthesis of penaresidin B is disclosed herein. The concise 8-step synthesis of azetidine aldehyde was devised by incorporating our novel strategy for ready access to 3-amino-2,3-dideoxysugars via regio- and stereoselective tandem hydroamination/glycosylation of glycal as the key step.
F. Ding, R. William, S. M. Kock, M. L. Leow and X. Liu, Chem. Commun., 2015, 51, 4639 DOI: 10.1039/C4CC09904D
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