Issue 14, 2016
From the journal:

Chemical Communications

Increasing the quantitative bandwidth of NMR measurements†

J. E. Power,a   M. Foroozandeh,a   R. W. Adams, ORCID logo a   M. Nilsson,a   S. R. Coombes,b   A. R. Phillipsb  and  G. A. Morris*a  

* Corresponding authors

a School of Chemistry, University of Manchester, Oxford Road, Manchester M13 9PL, UK
E-mail: g.a.morris@manchester.ac.uk

b Pharmaceutical Development, AstraZeneca, Silk Road Business Park, Macclesfield, UK

Abstract

The frequency range of quantitative NMR is increased from tens to hundreds of kHz by a new pulse sequence, CHORUS. It uses chirp pulses to excite uniformly over very large bandwidths, yielding accurate integrals even for nuclei such as 19F that have very wide spectra.

Graphical abstract: Increasing the quantitative bandwidth of NMR measurements

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Article information

DOI
https://doi.org/10.1039/C5CC10206E
Article type
Communication
Submitted
11 Dec 2015
Accepted
14 Jan 2016
First published
14 Jan 2016
This article is Open Access
Creative Commons BY license

Chem. Commun., 2016,52, 2916-2919

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Increasing the quantitative bandwidth of NMR measurements

J. E. Power, M. Foroozandeh, R. W. Adams, M. Nilsson, S. R. Coombes, A. R. Phillips and G. A. Morris, Chem. Commun., 2016, 52, 2916 DOI: 10.1039/C5CC10206E

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