Atomic positions and interactions between adsorbed guest molecules, such as ammonia in H-ZSM-5 microporous solids, are for the first time revealed by making use of the change in the periodical scattering parameter using in situ synchrotron powder X-ray diffraction combined with refinement within experimental errors.
L. Ye, B. T.W. Lo, J. Qu, I. Wilkinson, T. Hughes, C. A. Murray, C. C. Tang and S. C. E. Tsang, Chem. Commun., 2016, 52, 3422 DOI: 10.1039/C5CC10476A
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