We report an efficient catalytic method for the synthesis of mono-deuterated terminal alkynes directly from deuterium oxide, catalysed by a Ru(II) pincer complex in which the reaction proceeds via Ru–acetylide intermediates and amine–amide metal–ligand cooperation.
B. Chatterjee and C. Gunanathan, Chem. Commun., 2016, 52, 4509 DOI: 10.1039/C6CC01401A
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