A series of in situ hot stage experiments using transmission electron microscopy (TEM) were studied to directly observe the transition of a Ni-MOF to Ni nanoparticles wrapped in carbon (Ni-NPC) over temperatures ranging from ambient temperature to 700 °C. Ni-NPC-600 displays high catalytic activity in 4-nitrophenol reduction and high conversion, even after 10 cycles.
D. Xu, D. Zhang, H. Zou, L. Zhu, M. Xue, Q. Fang and S. Qiu, Chem. Commun., 2016, 52, 10513 DOI: 10.1039/C6CC05366A
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