Solvate crystals of 9,10-dimethyl-2,3,6,7,14,15-hexa(hydroxy)-triptycene (1) form a variety of 3D hydrogen-bonded topologies, including bcu, acs, bsn and an apparently new 7-connected net. Several of these networks contain 1D or 2D arrays of solvent-filled channels, amounting to up to 60% solvent-accessible void space.
S. Greatorex and M. A. Halcrow, CrystEngComm, 2016, 18, 4695 DOI: 10.1039/C6CE00966B
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