The combination of a palladium(II) precursor with a diimine–phenol ligand and an oxidant (H2O2 or O2) under different conditions has, serendipitously, given both a molecular square and a molecular tetrahedron by self-assembly of building blocks comprising palladium(II) centres coordinated to the oxidised forms of the ligand.
A. Behnia, P. D. Boyle, M. A. Fard, J. M. Blacquiere and R. J. Puddephatt, Dalton Trans., 2016, 45, 19485 DOI: 10.1039/C6DT04264C
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