Issue 65, 2017

Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

Abstract

2D double-quantum single-quantum correlation spectra with arbitrary spectral widths can be recorded with SR26 and related supercycled recoupling sequences when applying Supercycle-Timing-Compensation (STiC) phase shifts. This concept widely extends the applicability of supercycled sequences, most importantly for obtaining long-range distance constraints for structure determination with solid-state NMR.

Graphical abstract: Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

Supplementary files

Article information

Article type
Communication
Submitted
23 Jun 2017
Accepted
27 Jul 2017
First published
01 Aug 2017

Chem. Commun., 2017,53, 9155-9158

Efficient 2D double-quantum solid-state NMR spectroscopy with large spectral widths

K. Märker, S. Hediger and G. De Paëpe, Chem. Commun., 2017, 53, 9155 DOI: 10.1039/C7CC04890D

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