Hierarchical porous UiO-66-NH2 cm-monolithic xero- and aero-gels with a controlled shape and mechanical robustness were successfully produced from ethanolic gels. Their remarkable controlled hierarchical porosity was effectively assessed using N2 sorption, Hg intrusion porosimetry and focused ion beam-scanning electron microscopy methods.
S. M. F. Vilela, P. Salcedo-Abraira, L. Micheron, E. L. Solla, P. G. Yot and P. Horcajada, Chem. Commun., 2018, 54, 13088 DOI: 10.1039/C8CC07252C
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