The first expanded campestarenes based on a keto–enamine scaffold have been constructed using uranyl acetate as a template. Macrocycles with six and eight aryl rings in their backbone host dinuclear and tetranuclear uranium(VI) species, respectively. The complexes were characterized by SCXRD, FT-IR, UV-vis, and NMR spectroscopy, and DFT calculations corroborated their structures.
M. T. Chaudhry, F. Lelj and M. J. MacLachlan, Chem. Commun., 2018, 54, 11869 DOI: 10.1039/C8CC07269H
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