Direct synthesis of MoS2 or MoO3via thermolysis of a dialkyl dithiocarbamato molybdenum(IV) complex

Niting Zeng; David G. Hopkinson; Ben F. Spencer; Simon G. McAdams; Aleksander A. Tedstone; Sarah J. Haigh; David J. Lewis

doi:10.1039/C8CC08932A

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Direct synthesis of MoS₂ or MoO₃via thermolysis of a dialkyl dithiocarbamato molybdenum(iv) complex†

Niting Zeng,^a David G. Hopkinson,

^a Ben F. Spencer,

^a Simon G. McAdams,^a Aleksander A. Tedstone,^b Sarah J. Haigh

^a and David J. Lewis

*^a

Author affiliations

* Corresponding authors

^a School of Materials, University of Manchester, Oxford Road, UK
E-mail: david.lewis-4@manchester.ac.uk

^b School of Chemistry, University of Manchester, Oxford Road, UK

Abstract

Direct synthesis of either 2H-MoS₂ or α-MoO₃ is made possible by thermolysis of the same single source precursor in either argon or air at moderate temperatures.

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Article information

DOI: https://doi.org/10.1039/C8CC08932A
Article type: Communication
Submitted: 09 Nov 2018
Accepted: 29 Nov 2018
First published: 29 Nov 2018
This article is Open Access

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Chem. Commun., 2019,55, 99-102

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Direct synthesis of MoS₂ or MoO₃via thermolysis of a dialkyl dithiocarbamato molybdenum(IV) complex

N. Zeng, D. G. Hopkinson, B. F. Spencer, S. G. McAdams, A. A. Tedstone, S. J. Haigh and D. J. Lewis, Chem. Commun., 2019, 55, 99 DOI: 10.1039/C8CC08932A

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Chemical Communications