Microwave assisted combustion of phytic acid for the preparation of Ni2P@C as a robust catalyst for hydrodechlorination

Wenfeng Han; Xiliang Li; Bing Liu; Lichun Li; Haodong Tang; Ying Li; Chunshan Lu; Xiaonian Li

doi:10.1039/C9CC03479J

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Microwave assisted combustion of phytic acid for the preparation of Ni₂P@C as a robust catalyst for hydrodechlorination†

Wenfeng Han,

*^a Xiliang Li,^a Bing Liu,^a Lichun Li,^a Haodong Tang,^a Ying Li,

^a Chunshan Lu*^a and Xiaonian Li^a

Author affiliations

* Corresponding authors

^a Industrial Institute of Catalysis, Zhejiang University of Technology, Hangzhou, People's Republic of China
E-mail: hanwf@zjut.edu.cn, lcszjcn@zjut.edu.cn

Abstract

Ni₂P@C facilely prepared by microwave assisted combustion with phytic acid and nickel nitrate followed by reduction at 650 °C exhibits even higher activity for the hydrodechlorination of HCFC-22 than Pd/C. This method is also applicable for the synthesis of other metal phosphides, providing a versatile method for the fabrication of carbon encapsulated metal phosphide particles.

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Article information

DOI: https://doi.org/10.1039/C9CC03479J
Article type: Communication
Submitted: 06 May 2019
Accepted: 28 Jun 2019
First published: 01 Jul 2019

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Chem. Commun., 2019,55, 9279-9282

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Microwave assisted combustion of phytic acid for the preparation of Ni₂P@C as a robust catalyst for hydrodechlorination

W. Han, X. Li, B. Liu, L. Li, H. Tang, Y. Li, C. Lu and X. Li, Chem. Commun., 2019, 55, 9279 DOI: 10.1039/C9CC03479J

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