Issue 49, 2019
From the journal:

RSC Advances

Microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines: a rapid and efficient protocol for thioamides†

Jinyang Chen, ORCID logo a   Lan Mei,a   Jialing Liu,a   Chuntao Zhong,a   Binfang Yuan ORCID logo *a  and  Qiang Li ORCID logo b  

* Corresponding authors

a College of Chemistry and Chemical Engineering, Yangtze Normal University, Fuling, Chongqing, P. R. China
E-mail: 6781022@163.com

b Institution of Functional Organic Molecules and Materials, School of Chemistry and Chemical Engineering, Liaocheng University, No. 1, Hunan Street, Liaocheng, Shandong, P. R. China

Abstract

An efficient protocol for synthesis of thioamides was developed via the microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines. This process is scalable and tolerates a wide spectrum of amines to deliver the corresponding products in moderate to excellent yields in 10 minutes, providing a cheap and rapid approach to thioamides.

Graphical abstract: Microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines: a rapid and efficient protocol for thioamides

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Article information

DOI
https://doi.org/10.1039/C9RA05939C
Article type
Paper
Submitted
31 Jul 2019
Accepted
03 Sep 2019
First published
10 Sep 2019
This article is Open Access
Creative Commons BY-NC license

RSC Adv., 2019,9, 28576-28580

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Microwave-assisted iodine-catalyzed oxidative coupling of dibenzyl(difurfuryl)disulfides with amines: a rapid and efficient protocol for thioamides

J. Chen, L. Mei, J. Liu, C. Zhong, B. Yuan and Q. Li, RSC Adv., 2019, 9, 28576 DOI: 10.1039/C9RA05939C

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