New (triflyl)cyclobutenes have been prepared by palladium-catalyzed hydrodetriflylation reaction using water and deuterium oxide as convenient hydrogen and deuterium sources. In addition, an investigation of the possible mechanism for this Tsuji–Trost type reaction of bis(triflyl)cyclobutenes has been facilitated by labelling studies and density functional theory (DFT) calculations.
C. Lázaro-Milla, M. T. Quirós, D. J. Cárdenas and P. Almendros, Chem. Commun., 2020, 56, 6070 DOI: 10.1039/D0CC02146F
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